Information card for entry 2017830

Structure parameters

• Chemical name: [μ-hydrogen bis(<i>N</i>,<i>N</i>'-dioxidobutane-2,3-diimine)]tetrakis(1,10- phenanthroline)cobalt(III) trinitrate ethanol disolvate 1.87-hydrate
• Formula: C60 H60.74 Co2 N15 O16.87
• Calculated formula: C60 H60.744 Co2 N15 O16.864
• Title of publication: Two cobalt(III) mono-dimethylglyoximates isolated from one reaction
• Authors of publication: Czapik, Agnieszka; Gdaniec, Maria
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2010
• Journal volume: 66
• Journal issue: 9
• Pages of publication: m257 - m262
• a: 19.068 ± 0.0008 Å
• b: 16.017 ± 0.0005 Å
• c: 20.013 ± 0.0008 Å
• α: 90°
• β: 104.353 ± 0.004°
• γ: 90°
• Cell volume: 5921.4 ± 0.4 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0876
• Residual factor for significantly intense reflections: 0.0432
• Weighted residual factors for significantly intense reflections: 0.0868
• Weighted residual factors for all reflections included in the refinement: 0.0954
• Goodness-of-fit parameter for all reflections included in the refinement: 0.886
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes