Information card for entry 2017831

Structure parameters

• Chemical name: [<i>N</i>-hydroxy-<i>N</i>'-oxidobutane-2,3-diimine(1-)- κ^2^<i>N</i>,<i>N</i>']bis(1,10-phenanthroline- κ^2^<i>N</i>,<i>N</i>)cobalt(III) dinitrate ethanol monosolvate 0.4-hydrate
• Formula: C30 H29.8 Co N8 O9.4
• Calculated formula: C30 H29.403 Co N8 O9.403
• Title of publication: Two cobalt(III) mono-dimethylglyoximates isolated from one reaction
• Authors of publication: Czapik, Agnieszka; Gdaniec, Maria
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2010
• Journal volume: 66
• Journal issue: 9
• Pages of publication: m257 - m262
• a: 13.7587 ± 0.0001 Å
• b: 11.9763 ± 0.0001 Å
• c: 18.2055 ± 0.0002 Å
• α: 90°
• β: 96.744 ± 0.001°
• γ: 90°
• Cell volume: 2979.11 ± 0.05 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0438
• Residual factor for significantly intense reflections: 0.0381
• Weighted residual factors for significantly intense reflections: 0.1067
• Weighted residual factors for all reflections included in the refinement: 0.109
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes