Information card for entry 2019447

Structure parameters

• Chemical name: Bis{μ-<i>N</i>-[(diphenylphosphanyl)methyl]pyridin-4-amine-κ^2^<i>N</i>^1^:<i>P</i>}disilver bis(perchlorate) acetonitrile monosolvate
• Formula: C38 H37 Ag2 Cl2 N5 O8 P2
• Calculated formula: C38 H37 Ag2 Cl2 N5 O8 P2
• Title of publication: Counter-anion role in the formation of two supramolecular complexes: [Ag~2~(DPP)~2~](ClO~4~)~2~·CH~3~CN and [Ag~2~(DPP)~2~(NO~3~)~2~] {DPP is <i>N</i>-[(diphenylphosphanyl)methyl]pyridin-4-amine}
• Authors of publication: Liang, Guang-Ming; Shang, Jing; Yang, Kun-Guo; Ma, Kai; Ni, Qing-Ling
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2014
• Journal volume: 70
• Journal issue: 4
• Pages of publication: 379 - 383
• a: 11.928 ± 0.002 Å
• b: 18.192 ± 0.003 Å
• c: 19.026 ± 0.003 Å
• α: 90°
• β: 91.988 ± 0.003°
• γ: 90°
• Cell volume: 4126 ± 1.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0709
• Residual factor for significantly intense reflections: 0.0447
• Weighted residual factors for significantly intense reflections: 0.1226
• Weighted residual factors for all reflections included in the refinement: 0.1389
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes