In-house and synchrotron X-ray diffraction studies of 2-phenyl-1,10-phenanthroline, protonated salts, complexes with gold(III) and copper(II), and an orthometallation product with palladium(II)
Authors of publication
Krause, Jeanette A.; Zhao, Daoli; Chatterjee, Sayandev; Falcon, Roland; Stoltz, Kristen; Warren, John C.; Wiswell, Sara E.; Connick, William B.; Collins, Sibrina N.
Journal of publication
Acta Crystallographica Section C
Year of publication
2014
Journal volume
70
Journal issue
3
Pages of publication
260 - 266
a
7.5798 ± 0.0008 Å
b
10.693 ± 0.0012 Å
c
10.9157 ± 0.0012 Å
α
103.713 ± 0.003°
β
90.801 ± 0.003°
γ
104.707 ± 0.003°
Cell volume
828.75 ± 0.16 Å3
Cell temperature
173 ± 2 K
Ambient diffraction temperature
173 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0664
Residual factor for significantly intense reflections
0.0586
Weighted residual factors for significantly intense reflections
0.1657
Weighted residual factors for all reflections included in the refinement
0.1736
Goodness-of-fit parameter for all reflections included in the refinement
