In-house and synchrotron X-ray diffraction studies of 2-phenyl-1,10-phenanthroline, protonated salts, complexes with gold(III) and copper(II), and an orthometallation product with palladium(II)
Authors of publication
Krause, Jeanette A.; Zhao, Daoli; Chatterjee, Sayandev; Falcon, Roland; Stoltz, Kristen; Warren, John C.; Wiswell, Sara E.; Connick, William B.; Collins, Sibrina N.
Journal of publication
Acta Crystallographica Section C
Year of publication
2014
Journal volume
70
Journal issue
3
Pages of publication
260 - 266
a
7.6682 ± 0.0002 Å
b
10.7446 ± 0.0004 Å
c
11.1174 ± 0.0004 Å
α
104.848 ± 0.002°
β
95.687 ± 0.002°
γ
100.439 ± 0.002°
Cell volume
860.48 ± 0.05 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0391
Residual factor for significantly intense reflections
0.0352
Weighted residual factors for significantly intense reflections
0.0984
Weighted residual factors for all reflections included in the refinement
0.1022
Goodness-of-fit parameter for all reflections included in the refinement
