Hydrogen-bonded chains in 3,5-bis(4-fluorophenyl)-1-phenyl-1<i>H</i>-pyrazole and complex hydrogen-bonded sheets in (5<i>RS</i>,6<i>SR</i>)-6-(4-fluorobenzoyl)-5-(4-fluorophenyl)-2-(4-hydroxyphenyl)-5,6-dihydro-4<i>H</i>-1,3,4-oxadiazine <i>N</i>,<i>N</i>-dimethylformamide monosolvate
Authors of publication
Samshuddin, Seranthimata; Jasinski, Jerry P.; Golen, James A.; Narayana, Badiadka; Yathirajan, Hemmige S.; Glidewell, Christopher
Journal of publication
Acta Crystallographica Section C
Year of publication
2014
Journal volume
70
Journal issue
9
a
31.729 ± 0.002 Å
b
10.4118 ± 0.0007 Å
c
10.1697 ± 0.0006 Å
α
90°
β
97.7 ± 0.007°
γ
90°
Cell volume
3329.3 ± 0.4 Å3
Cell temperature
123 ± 2 K
Ambient diffraction temperature
123 ± 2 K
Number of distinct elements
4
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.0722
Residual factor for significantly intense reflections
0.066
Weighted residual factors for significantly intense reflections
0.1676
Weighted residual factors for all reflections included in the refinement
0.1744
Goodness-of-fit parameter for all reflections included in the refinement
