Hydrogen-bonded chains in 3,5-bis(4-fluorophenyl)-1-phenyl-1<i>H</i>-pyrazole and complex hydrogen-bonded sheets in (5<i>RS</i>,6<i>SR</i>)-6-(4-fluorobenzoyl)-5-(4-fluorophenyl)-2-(4-hydroxyphenyl)-5,6-dihydro-4<i>H</i>-1,3,4-oxadiazine <i>N</i>,<i>N</i>-dimethylformamide monosolvate
Authors of publication
Samshuddin, Seranthimata; Jasinski, Jerry P.; Golen, James A.; Narayana, Badiadka; Yathirajan, Hemmige S.; Glidewell, Christopher
Journal of publication
Acta Crystallographica Section C
Year of publication
2014
Journal volume
70
Journal issue
9
a
17.5182 ± 0.0007 Å
b
7.4306 ± 0.0003 Å
c
17.5595 ± 0.0007 Å
α
90°
β
101.252 ± 0.004°
γ
90°
Cell volume
2241.8 ± 0.16 Å3
Cell temperature
173 ± 2 K
Ambient diffraction temperature
173 ± 2 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0525
Residual factor for significantly intense reflections
0.0477
Weighted residual factors for significantly intense reflections
0.1372
Weighted residual factors for all reflections included in the refinement
0.1474
Goodness-of-fit parameter for all reflections included in the refinement
