Information card for entry 2020678

Structure parameters

• Chemical name: {2,4-Di-<i>tert-butyl</i>-6-[(2,6-diisopropylphenyl)iminomethyl]phenolato-κ^2^<i>N</i>,<i>O</i>}bis(pyridine-κ<i>N</i>)magnesium(II) toluene monosolvate
• Formula: C69 H91 Mg N5 O2
• Calculated formula: C69 H91 Mg N5 O2
• Title of publication: Solvent dependence of the solid-state structures of salicylaldiminate magnesium amide complexes
• Authors of publication: Rood, Jeffrey A.; Landis, Ashley M.; Forster, Daniel R.; Goldkamp, Timothy; Oliver, Allen G.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2016
• Journal volume: 72
• Journal issue: 12
• Pages of publication: 990 - 996
• a: 31.633 ± 0.004 Å
• b: 13.4541 ± 0.0015 Å
• c: 17.467 ± 0.003 Å
• α: 90°
• β: 122.934 ± 0.003°
• γ: 90°
• Cell volume: 6239.2 ± 1.5 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0835
• Residual factor for significantly intense reflections: 0.0524
• Weighted residual factors for significantly intense reflections: 0.1176
• Weighted residual factors for all reflections included in the refinement: 0.1361
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes