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Information card for entry 2023038
Preview
Coordinates | 2023038.cif |
---|---|
Structure factors | 2023038.hkl |
Original IUCr paper | HTML |
Common name | Bis[1-oxopyridin-2-olato(1-)]bis(pentafluorophenyl)silicon(IV)–tetrahydrofuran–pentane (2/1/1) |
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Chemical name | Bis[1-oxopyridin-2-olato(1-)]bis(pentafluorophenyl)silicon(IV)–tetrahydrofuran–pentane (2/1/1) |
Formula | C26.5 H18 F10 N2 O4.5 Si |
Calculated formula | C26.5 H18 F10 N2 O4.5 Si |
Title of publication | Synthesis and crystal structures of bis-[1-oxopyridin-2-olato(1-)]bis-(penta-fluoro-phen-yl)silicon(IV)-tetra-hydro-furan-pentane (2/1/1), bis-[1-oxopyridin-2-olato(1-)]bis-(<i>p</i>-tol-yl)silicon(IV), and dimesitylbis[1-oxopyridin-2-olato(1-)]silicon(IV). |
Authors of publication | Kraft, Bradley M.; Brennessel, William W.; Andrews, Jordan W.; Viggiani, Michael T.; Kittrell, Nathan F.; Heckman, Matthew T. |
Journal of publication | Acta crystallographica. Section E, Crystallographic communications |
Year of publication | 2024 |
Journal volume | 80 |
Journal issue | Pt 3 |
Pages of publication | 318 - 324 |
a | 12.6809 ± 0.0009 Å |
b | 12.1217 ± 0.0009 Å |
c | 17.7335 ± 0.0013 Å |
α | 90° |
β | 105.767 ± 0.0015° |
γ | 90° |
Cell volume | 2623.3 ± 0.3 Å3 |
Cell temperature | 100 ± 0.5 K |
Ambient diffraction temperature | 100 ± 0.5 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0817 |
Residual factor for significantly intense reflections | 0.0513 |
Weighted residual factors for significantly intense reflections | 0.1448 |
Weighted residual factors for all reflections included in the refinement | 0.1629 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.033 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | Yes |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/2023038.html
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Users of the data should acknowledge the original authors of the
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