Crystal Engineering Using Bisphenols and Trisphenols. Complexes with Hexamethylenetetramine (HMTA): Strings, Multiple Helices and Chains-of-Rings in the Crystal Structures of the Adducts of HTMA with 4,4'-Thiodiphenol (1/1), 4,4'-Sulfonyldiphenol (1/1), 4,4'-Isopropylidenediphenol (1/1), 1,1,1-Tris(4-hydroxyphenyl)ethane (1/2) and 1,3,5-Trihydroxybenzene (2/3)
Authors of publication
Ferguson, George
Journal of publication
Acta Crystallographica Section B
Year of publication
1997
Journal volume
53
Journal issue
3
Pages of publication
521 - 533
a
14.779 ± 0.002 Å
b
10.2558 ± 0.0015 Å
c
5.9817 ± 0.0008 Å
α
90°
β
90°
γ
90°
Cell volume
906.6 ± 0.2 Å3
Cell temperature
294 ± 1 K
Ambient diffraction temperature
294 ± 1 K
Number of distinct elements
5
Space group number
31
Hermann-Mauguin space group symbol
P m n 21
Hall space group symbol
P 2ac -2
Residual factor for all reflections
0.0682
Residual factor for significantly intense reflections
0.0421
Weighted residual factors for all reflections
0.0947
Weighted residual factors for significantly intense reflections
0.0885
Goodness-of-fit parameter for all reflections
1.034
Goodness-of-fit parameter for significantly intense reflections
