Crystal Engineering Using Bisphenols and Trisphenols. Complexes with Hexamethylenetetramine (HMTA): Strings, Multiple Helices and Chains-of-Rings in the Crystal Structures of the Adducts of HTMA with 4,4'-Thiodiphenol (1/1), 4,4'-Sulfonyldiphenol (1/1), 4,4'-Isopropylidenediphenol (1/1), 1,1,1-Tris(4-hydroxyphenyl)ethane (1/2) and 1,3,5-Trihydroxybenzene (2/3)
Authors of publication
Ferguson, George
Journal of publication
Acta Crystallographica Section B
Year of publication
1997
Journal volume
53
Journal issue
3
Pages of publication
521 - 533
a
25.093 ± 0.006 Å
b
7.1742 ± 0.0013 Å
c
23.612 ± 0.007 Å
α
90°
β
110.42 ± 0.02°
γ
90°
Cell volume
3983.6 ± 1.8 Å3
Cell temperature
294 ± 1 K
Ambient diffraction temperature
294 ± 1 K
Number of distinct elements
4
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.1461
Residual factor for significantly intense reflections
0.0401
Weighted residual factors for all reflections
0.1027
Weighted residual factors for significantly intense reflections
0.085
Goodness-of-fit parameter for all reflections
0.913
Goodness-of-fit parameter for significantly intense reflections
