Metal distribution and disorder in the crystal structure of [NH~2~Et~2~][Cr~7~<i>M</i>F~8~(^<i>t^</i>BuCO~2~)~16~] wheel molecules for <i>M</i> = Mn, Fe, Co, Ni, Cu, Zn and Cd
Authors of publication
Larsen, Finn Krebs; Overgaard, Jacob; Christensen, Mogens; McIntyre, Garry James; Timco, Grigore; Winpenny, Richard E. P.
Journal of publication
Acta Crystallographica Section B
Year of publication
2014
Journal volume
70
Journal issue
6
Pages of publication
932 - 941
a
25.0491 ± 0.0015 Å
b
16.6301 ± 0.001 Å
c
30.9272 ± 0.0018 Å
α
90°
β
110.183 ± 0.001°
γ
90°
Cell volume
12092.2 ± 1.2 Å3
Cell temperature
120 ± 2 K
Ambient diffraction temperature
120 ± 2 K
Number of distinct elements
7
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0959
Residual factor for significantly intense reflections
0.0587
Weighted residual factors for significantly intense reflections
0.1594
Weighted residual factors for all reflections included in the refinement
0.1801
Goodness-of-fit parameter for all reflections included in the refinement
