Metal distribution and disorder in the crystal structure of [NH~2~Et~2~][Cr~7~<i>M</i>F~8~(^<i>t^</i>BuCO~2~)~16~] wheel molecules for <i>M</i> = Mn, Fe, Co, Ni, Cu, Zn and Cd
Authors of publication
Larsen, Finn Krebs; Overgaard, Jacob; Christensen, Mogens; McIntyre, Garry James; Timco, Grigore; Winpenny, Richard E. P.
Journal of publication
Acta Crystallographica Section B
Year of publication
2014
Journal volume
70
Journal issue
6
Pages of publication
932 - 941
a
25.0305 ± 0.0013 Å
b
16.6392 ± 0.0009 Å
c
30.9101 ± 0.0016 Å
α
90°
β
110.025 ± 0.001°
γ
90°
Cell volume
12095.4 ± 1.1 Å3
Cell temperature
153 ± 2 K
Ambient diffraction temperature
153 ± 2 K
Number of distinct elements
7
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0764
Residual factor for significantly intense reflections
0.053
Weighted residual factors for significantly intense reflections
0.1462
Weighted residual factors for all reflections included in the refinement
0.1609
Goodness-of-fit parameter for all reflections included in the refinement
