Metal distribution and disorder in the crystal structure of [NH~2~Et~2~][Cr~7~<i>M</i>F~8~(^<i>t^</i>BuCO~2~)~16~] wheel molecules for <i>M</i> = Mn, Fe, Co, Ni, Cu, Zn and Cd
Authors of publication
Larsen, Finn Krebs; Overgaard, Jacob; Christensen, Mogens; McIntyre, Garry James; Timco, Grigore; Winpenny, Richard E. P.
Journal of publication
Acta Crystallographica Section B
Year of publication
2014
Journal volume
70
Journal issue
6
Pages of publication
932 - 941
a
24.8611 ± 0.0016 Å
b
16.5028 ± 0.0012 Å
c
30.85 ± 0.002 Å
α
90°
β
110.092 ± 0.003°
γ
90°
Cell volume
11886.8 ± 1.4 Å3
Cell temperature
273 ± 2 K
Ambient diffraction temperature
273 ± 2 K
Number of distinct elements
7
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0887
Residual factor for significantly intense reflections
0.0589
Weighted residual factors for significantly intense reflections
0.1368
Weighted residual factors for all reflections included in the refinement
0.1587
Goodness-of-fit parameter for all reflections included in the refinement
