Information card for entry 2202279

Structure parameters

• Common name: μ-OH [Re(dmbpy)(CO)~3~]~2~ ReO~4~ acetone solvate
• Chemical name: μ-Hydroxo bis-[Tricarbonyl(4,4'-dimethyl-2,2'-bipyridine) rhenium(I)] perrhenate acetone solvate
• Formula: C31.5 H28 N4 O11.5 Re3
• Calculated formula: C31.5 H25 N4 O11.5 Re3
• Title of publication: μ-Hydroxo-bis[(4,4'-dimethyl-2,2'-bipyridine)tricarbonylrhenium(I)] perrhenate acetone hemisolvate
• Authors of publication: Gibson, Dorothy H.; Mashuta, Mark S.; Yin, Xiaolong
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2003
• Journal volume: 59
• Journal issue: 10
• Pages of publication: m911 - m913
• a: 10.6841 ± 0.0007 Å
• b: 31.649 ± 0.002 Å
• c: 10.5758 ± 0.0007 Å
• α: 90°
• β: 105.222 ± 0.001°
• γ: 90°
• Cell volume: 3450.6 ± 0.4 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.032
• Residual factor for significantly intense reflections: 0.027
• Weighted residual factors for significantly intense reflections: 0.074
• Weighted residual factors for all reflections included in the refinement: 0.076
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes