A tetrakis(secondary amide) derivative of quadricyclane: 3-isopropylidenetetracyclo[3.2.0.0^2,7^.0^4,6^]heptane-1,5,6,7-tetracarboxylic acid tetrakis(cyclohexylamide)
Authors of publication
Winkler, Torsten; Herges, Rainer; Jones, Peter G.; Dix, Ina
Journal of publication
Acta Crystallographica Section E
Year of publication
2003
Journal volume
59
Journal issue
8
Pages of publication
o1098 - o1100
a
10.1995 ± 0.0014 Å
b
11.6467 ± 0.0016 Å
c
15.206 ± 0.002 Å
α
87.126 ± 0.003°
β
77.132 ± 0.003°
γ
81.3 ± 0.003°
Cell volume
1740.4 ± 0.4 Å3
Cell temperature
143 ± 2 K
Ambient diffraction temperature
143 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0613
Residual factor for significantly intense reflections
0.0385
Weighted residual factors for significantly intense reflections
0.0952
Weighted residual factors for all reflections included in the refinement
0.1051
Goodness-of-fit parameter for all reflections included in the refinement
