Information card for entry 2219677

Structure parameters

• Chemical name: μ-Squarato-κ^2^O^1^:O^2^-bis{[2-(2-aminoethyl)pyridine- κ^2^N,N']aquanickel(II)} squarate 0.25-hydrate
• Formula: C36 H44 N8 Ni2 O10.25
• Calculated formula: C36 H44 N8 Ni2 O10.25
• Title of publication: μ-Squarato-κ^2^<i>O</i>^1^:<i>O</i>^2^-bis{[2-(2-aminoethyl)pyridine-κ^2^<i>N</i>,<i>N</i>']aquanickel(II)} squarate 0.25-hydrate
• Authors of publication: Bekdemir, Yunus; Uçar, Ibrahim; Büyükgüngör, Orhan
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 10
• Pages of publication: m1344 - m1345
• a: 28.037 ± 0.003 Å
• b: 8.0409 ± 0.0005 Å
• c: 17.7752 ± 0.0016 Å
• α: 90°
• β: 103.572 ± 0.007°
• γ: 90°
• Cell volume: 3895.4 ± 0.6 ų
• Cell temperature: 297 ± 2 K
• Ambient diffraction temperature: 297 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0386
• Residual factor for significantly intense reflections: 0.0289
• Weighted residual factors for significantly intense reflections: 0.0697
• Weighted residual factors for all reflections included in the refinement: 0.0728
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes