6,7,9,10-Tetrahydro-16,22-ethanooxyethano-5,8,11,19-tetraoxa-16,22-diazadibenzo[<i>h</i>,<i>q</i>]cyclooctadecine-17,21-dione: a benzylannelated macrobicyclic diamide
Authors of publication
Smith, Gary L. N.; Lei, Yang; Powell, Douglas R.; Taylor, Richard W.
Journal of publication
Acta Crystallographica Section E
Year of publication
2008
Journal volume
64
Journal issue
10
Pages of publication
o2003
a
15.125 ± 0.002 Å
b
9.3901 ± 0.0014 Å
c
16.446 ± 0.002 Å
α
90°
β
108.416 ± 0.005°
γ
90°
Cell volume
2216.1 ± 0.5 Å3
Cell temperature
87 ± 2 K
Ambient diffraction temperature
87 ± 2 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0337
Residual factor for significantly intense reflections
0.0324
Weighted residual factors for significantly intense reflections
0.0837
Weighted residual factors for all reflections included in the refinement
0.0848
Goodness-of-fit parameter for all reflections included in the refinement