Information card for entry 2226290

Structure parameters

• Chemical name: Ethylenediammonium tetrakis({2,2'-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato}nickel(II)) bis(perchlorate) dimethylformamide monosolvate
• Formula: C69 H73 Cl2 N11 Ni4 O17
• Calculated formula: C69 H73 Cl2 N11 Ni4 O17
• Title of publication: Ethylenediammonium tetrakis({2,2'-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato}nickel(II)) bis(perchlorate) dimethylformamide monosolvate
• Authors of publication: Assey, Gervas; Gultneh, Yilma; Butcher, Ray J.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2010
• Journal volume: 66
• Journal issue: 6
• Pages of publication: m654 - m655
• a: 15.0209 ± 0.0011 Å
• b: 15.0492 ± 0.0013 Å
• c: 18.2709 ± 0.0008 Å
• α: 85.99 ± 0.005°
• β: 86.506 ± 0.005°
• γ: 62.963 ± 0.008°
• Cell volume: 3667.8 ± 0.5 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0577
• Residual factor for significantly intense reflections: 0.0389
• Weighted residual factors for significantly intense reflections: 0.1045
• Weighted residual factors for all reflections included in the refinement: 0.1096
• Goodness-of-fit parameter for all reflections included in the refinement: 0.954
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes