Information card for entry 2229412

Structure parameters

• Chemical name: Di-μ~2~-methoxo-bis{[μ-3,10,18,25-tetraazapentacyclo[17.4.4.3.1.1]triconta- 1(31),2,4(9),5,7,10,12,14,16(32),17,19(24),20,22,25,27,29-hexadecaene-31,32- diolato]dizinc(II)} bis(perchlorate) <i>N</i>,<i>N</i>-dimethylformamide disolvate
• Formula: C64 H56 Cl2 N10 O16 Zn4
• Calculated formula: C64 H56 Cl2 N10 O16 Zn4
• Title of publication: Di-μ~2~-methoxo-bis{[μ-3,10,18,25-tetraazapentacyclo[17.4.4.3.1.1]triconta-1(31),2,4(9),5,7,10,12,14,16(32),17,19(24),20,22,25,27,29-hexadecaene-31,32-diolato]dizinc(II)} bis(perchlorate) <i>N</i>,<i>N</i>-dimethylformamide disolvate
• Authors of publication: Lim, Zelong; Forsyth, Craig M.; Graham, Bim
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2011
• Journal volume: 67
• Journal issue: 3
• Pages of publication: m368
• a: 30.9454 ± 0.0004 Å
• b: 10.4512 ± 0.0002 Å
• c: 20.5774 ± 0.0004 Å
• α: 90°
• β: 112.019 ± 0.001°
• γ: 90°
• Cell volume: 6169.65 ± 0.19 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0762
• Residual factor for significantly intense reflections: 0.0448
• Weighted residual factors for significantly intense reflections: 0.1072
• Weighted residual factors for all reflections included in the refinement: 0.1228
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes