Information card for entry 2232551

Structure parameters

• Chemical name: <i>cyclo</i>-Tetra-μ-oxido-tetrakis[(acetylacetonato- κ^2^<i>O</i>,<i>O</i>')bis(ethanolato-κ<i>O</i>)niobium(V)]
• Formula: C36 H68 Nb4 O20
• Calculated formula: C36 H68 Nb4 O20
• Title of publication: <i>cyclo</i>-Tetra-μ-oxido-tetrakis[(acetylacetonato-κ^2^<i>O</i>,<i>O</i>')bis(ethanolato-κ<i>O</i>)niobium(V)]
• Authors of publication: Herbst, Leandra; Visser, Hendrik G.; Roodt, Andreas; Muller, Theunis J.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2011
• Journal volume: 67
• Journal issue: 12
• Pages of publication: m1669 - m1670
• a: 13.907 ± 0.005 Å
• b: 12.662 ± 0.005 Å
• c: 21.354 ± 0.005 Å
• α: 90°
• β: 136.982 ± 0.013°
• γ: 90°
• Cell volume: 2565.3 ± 1.6 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0389
• Residual factor for significantly intense reflections: 0.0309
• Weighted residual factors for all reflections included in the refinement: 0.0796
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes