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Information card for entry 4027892
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Coordinates | 4027892.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C19 H33 N O3.1 Si |
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Calculated formula | C19 H33 N O3.098 Si |
Title of publication | Total Synthesis of the Lycopodium Alkaloid Serratezomine A Using Free Radical-Mediated Vinyl Amination to Prepare a β-Stannyl Enamine Linchpin |
Authors of publication | Julie A. Pigza; Jeong-Seok Han; Aroop Chandra; Daniel Mutnick; Maren Pink; Jeffrey N. Johnston |
Journal of publication | Journal of Organic Chemistry |
Year of publication | 2013 |
Journal volume | 78 |
Pages of publication | 822 - 843 |
a | 24.705 ± 0.009 Å |
b | 6.725 ± 0.003 Å |
c | 11.915 ± 0.004 Å |
α | 90° |
β | 97.458 ± 0.009° |
γ | 90° |
Cell volume | 1962.8 ± 1.3 Å3 |
Cell temperature | 117 ± 2 K |
Ambient diffraction temperature | 117 ± 2 K |
Number of distinct elements | 5 |
Space group number | 5 |
Hermann-Mauguin space group symbol | C 1 2 1 |
Hall space group symbol | C 2y |
Residual factor for all reflections | 0.0482 |
Residual factor for significantly intense reflections | 0.0373 |
Weighted residual factors for significantly intense reflections | 0.0793 |
Weighted residual factors for all reflections included in the refinement | 0.0845 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.024 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4027892.html
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