Crystallography Open Database

Information card for entry 4027893

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Coordinates	4027893.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H50 F3 N O7 S Si
Calculated formula	C28 H50 F3 N O7 S Si
Title of publication	Total Synthesis of the Lycopodium Alkaloid Serratezomine A Using Free Radical-Mediated Vinyl Amination to Prepare a β-Stannyl Enamine Linchpin
Authors of publication	Julie A. Pigza; Jeong-Seok Han; Aroop Chandra; Daniel Mutnick; Maren Pink; Jeffrey N. Johnston
Journal of publication	Journal of Organic Chemistry
Year of publication	2013
Journal volume	78
Pages of publication	822 - 843
a	7.8828 ± 0.0004 Å
b	10.6926 ± 0.0005 Å
c	20.2725 ± 0.0009 Å
α	105.055 ± 0.001°
β	92.644 ± 0.001°
γ	94.146 ± 0.001°
Cell volume	1642.01 ± 0.14 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	1
Hermann-Mauguin space group symbol	P 1
Hall space group symbol	P 1
Residual factor for all reflections	0.0557
Residual factor for significantly intense reflections	0.0424
Weighted residual factors for significantly intense reflections	0.1076
Weighted residual factors for all reflections included in the refinement	0.1203
Goodness-of-fit parameter for all reflections included in the refinement	1.07
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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