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Information card for entry 4030337
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Coordinates | 4030337.cif |
---|
Formula | C76 H68 B Cl O P4 W |
---|---|
Calculated formula | C76 B Cl O P4 W |
Title of publication | Oxohalo complexes of W (V) and W (IV). The synthesis od crystal structures of [WOCl (dppe)2][BPh4], [PHMe2Ph][WOBr4(OPMe2Ph)] and [Li(OPMe2Ph)(THF)]2[WOBr4(OPMe2Ph)]2 |
Authors of publication | Cotton, F. A.; Mandal, S. K. |
Journal of publication | European Journal of Solid State and Inorganic Chemistry |
Year of publication | 1991 |
Journal volume | 28 |
Pages of publication | 775 - 797 |
a | 10.291 ± 0.003 Å |
b | 24.274 ± 0.009 Å |
c | 26.07 ± 0.01 Å |
α | 90° |
β | 96.09 ± 0.03° |
γ | 90° |
Cell volume | 6476 ± 4 Å3 |
Ambient diffraction temperature | 294 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for significantly intense reflections | 0.074 |
Weighted residual factors for significantly intense reflections | 0.092 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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