Crystallography Open Database

Information card for entry 4036516

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Coordinates	4036516.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H30 O6 Rh S
Calculated formula	C24 H27.36 O6 Rh S
Title of publication	Dirhodium(II)-Catalyzed Sulfide Oxygenations: Catalyst Removal by Coprecipitation with Sulfoxides.
Authors of publication	Zhao, Lili; Zhang, Hongyang; Wang, Yuanhua
Journal of publication	The Journal of organic chemistry
Year of publication	2016
Journal volume	81
Journal issue	1
Pages of publication	129 - 136
a	13.9681 ± 0.0002 Å
b	10.30952 ± 0.00019 Å
c	17.1108 ± 0.0003 Å
α	90°
β	92.2033 ± 0.0016°
γ	90°
Cell volume	2462.21 ± 0.07 Å³
Cell temperature	293 K
Ambient diffraction temperature	293 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0716
Residual factor for significantly intense reflections	0.0426
Weighted residual factors for significantly intense reflections	0.086
Weighted residual factors for all reflections included in the refinement	0.0935
Goodness-of-fit parameter for all reflections included in the refinement	1.112
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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