Crystallography Open Database

Information card for entry 4036517

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Coordinates	4036517.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H40 O8 Rh S2
Calculated formula	C32 H40 O8 Rh S2
Title of publication	Dirhodium(II)-Catalyzed Sulfide Oxygenations: Catalyst Removal by Coprecipitation with Sulfoxides.
Authors of publication	Zhao, Lili; Zhang, Hongyang; Wang, Yuanhua
Journal of publication	The Journal of organic chemistry
Year of publication	2016
Journal volume	81
Journal issue	1
Pages of publication	129 - 136
a	11.4979 ± 0.0003 Å
b	11.639 ± 0.0002 Å
c	14.4566 ± 0.0003 Å
α	113.631 ± 0.0018°
β	98.7999 ± 0.0018°
γ	106.77 ± 0.0018°
Cell volume	1615.5 ± 0.07 Å³
Cell temperature	208.26 ± 0.1 K
Ambient diffraction temperature	208.26 ± 0.1 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0392
Residual factor for significantly intense reflections	0.0333
Weighted residual factors for significantly intense reflections	0.0748
Weighted residual factors for all reflections included in the refinement	0.0783
Goodness-of-fit parameter for all reflections included in the refinement	1.05
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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