Information card for entry 4037700
Formula |
C23 H20 N2 O |
Calculated formula |
C23 H20 N2 O |
SMILES |
N1(CN(CC(=C1)C(=O)c1ccccc1)c1ccccc1)c1ccccc1 |
Title of publication |
One-pot Methylenation-Cyclization Employing Two Molecules of CO2 with Arylamines and Enaminones. |
Authors of publication |
Zhao, Yulei; Liu, Xu; Zheng, Lijun; Du, Yulan; Shi, Xinrui; Liu, Yunlin; Yan, Zhengquan; You, Jinmao; Jiang, Yuan-Ye |
Journal of publication |
The Journal of organic chemistry |
Year of publication |
2019 |
a |
10.573 ± 0.0009 Å |
b |
16.5389 ± 0.0014 Å |
c |
20.6478 ± 0.0018 Å |
α |
90° |
β |
90.648 ± 0.002° |
γ |
90° |
Cell volume |
3610.4 ± 0.5 Å3 |
Cell temperature |
298 ± 2 K |
Ambient diffraction temperature |
298 ± 2 K |
Number of distinct elements |
4 |
Space group number |
15 |
Hermann-Mauguin space group symbol |
C 1 2/c 1 |
Hall space group symbol |
-C 2yc |
Residual factor for all reflections |
0.1012 |
Residual factor for significantly intense reflections |
0.0519 |
Weighted residual factors for significantly intense reflections |
0.1367 |
Weighted residual factors for all reflections included in the refinement |
0.1555 |
Goodness-of-fit parameter for all reflections included in the refinement |
1.06 |
Diffraction radiation wavelength |
0.71073 Å |
Diffraction radiation type |
MoKα |
Has coordinates |
Yes |
Has disorder |
No |
Has Fobs |
No |
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https://www.crystallography.net/4037700.html