Information card for entry 4037701
Formula |
C24 H21 N3 O3 |
Calculated formula |
C24 H21 N3 O3 |
Title of publication |
One-pot Methylenation-Cyclization Employing Two Molecules of CO2 with Arylamines and Enaminones. |
Authors of publication |
Zhao, Yulei; Liu, Xu; Zheng, Lijun; Du, Yulan; Shi, Xinrui; Liu, Yunlin; Yan, Zhengquan; You, Jinmao; Jiang, Yuan-Ye |
Journal of publication |
The Journal of organic chemistry |
Year of publication |
2019 |
a |
8.3991 ± 0.0006 Å |
b |
8.9 ± 0.0007 Å |
c |
14.7773 ± 0.0012 Å |
α |
100.999 ± 0.002° |
β |
98.098 ± 0.002° |
γ |
106.921 ± 0.003° |
Cell volume |
1014.46 ± 0.14 Å3 |
Cell temperature |
298 ± 2 K |
Ambient diffraction temperature |
298 ± 2 K |
Number of distinct elements |
4 |
Space group number |
2 |
Hermann-Mauguin space group symbol |
P -1 |
Hall space group symbol |
-P 1 |
Residual factor for all reflections |
0.0845 |
Residual factor for significantly intense reflections |
0.0486 |
Weighted residual factors for significantly intense reflections |
0.1089 |
Weighted residual factors for all reflections included in the refinement |
0.1207 |
Goodness-of-fit parameter for all reflections included in the refinement |
1.036 |
Diffraction radiation wavelength |
0.71073 Å |
Diffraction radiation type |
MoKα |
Has coordinates |
Yes |
Has disorder |
Yes |
Has Fobs |
No |
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https://www.crystallography.net/4037701.html