Information card for entry 4038392

Structure parameters

• Formula: C22 H17 F O4 S
• Calculated formula: C22 H17 F O4 S
• Title of publication: CuBr₂-Mediated One-Pot Synthesis of Sulfonyl 9-Fluorenylidenes.
• Authors of publication: Chang, Meng-Yang; Tsai, Yu-Lin; Chen, Hsing-Yin
• Journal of publication: The Journal of organic chemistry
• Year of publication: 2020
• a: 8.3081 ± 0.0003 Å
• b: 10.2495 ± 0.0003 Å
• c: 20.9221 ± 0.0007 Å
• α: 90°
• β: 94.604 ± 0.002°
• γ: 90°
• Cell volume: 1775.85 ± 0.1 ų
• Cell temperature: 99 ± 2 K
• Ambient diffraction temperature: 99 ± 2 K
• Number of distinct elements: 5
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/c 1
• Hall space group symbol: -P 2yc
• Residual factor for all reflections: 0.0615
• Residual factor for significantly intense reflections: 0.0448
• Weighted residual factors for significantly intense reflections: 0.1119
• Weighted residual factors for all reflections included in the refinement: 0.121
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No