Information card for entry 4038393

Structure parameters

• Formula: C30 H28 O6 S2
• Calculated formula: C30 H28 O6 S2
• Title of publication: CuBr₂-Mediated One-Pot Synthesis of Sulfonyl 9-Fluorenylidenes.
• Authors of publication: Chang, Meng-Yang; Tsai, Yu-Lin; Chen, Hsing-Yin
• Journal of publication: The Journal of organic chemistry
• Year of publication: 2020
• a: 20.676 ± 0.002 Å
• b: 14.0649 ± 0.0014 Å
• c: 9.2725 ± 0.0008 Å
• α: 90°
• β: 101.965 ± 0.004°
• γ: 90°
• Cell volume: 2637.9 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1252
• Residual factor for significantly intense reflections: 0.0982
• Weighted residual factors for significantly intense reflections: 0.2655
• Weighted residual factors for all reflections included in the refinement: 0.2791
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No