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Information card for entry 4038972
Preview
Coordinates | 4038972.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C26 H29 Mo2 O7 P W |
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Calculated formula | C26 H29 Mo2 O7 P W |
Title of publication | Reactions of the unsaturated methyl-bridged complexes [Mo2Cp2(μ-CH3)(μ-P Bu2)(CO)x] (x = 1, 2) towards transition metal carbonyls: convenient dehydrogenative route to heterometallic methylidyne-bridged clusters |
Authors of publication | Alvarez, M. Angeles; Casado-Ruano, Melodie; García, M. Esther; García-Vivó, Daniel; Ruiz, Miguel A. |
Journal of publication | Journal of Organometallic Chemistry |
Year of publication | 2022 |
Journal volume | 959 |
Pages of publication | 122206 |
a | 10.4841 ± 0.0001 Å |
b | 20.5016 ± 0.0002 Å |
c | 13.3506 ± 0.0001 Å |
α | 90° |
β | 105.05 ± 0.001° |
γ | 90° |
Cell volume | 2771.16 ± 0.05 Å3 |
Cell temperature | 152 ± 3 K |
Ambient diffraction temperature | 152 ± 3 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0281 |
Residual factor for significantly intense reflections | 0.0255 |
Weighted residual factors for significantly intense reflections | 0.0615 |
Weighted residual factors for all reflections included in the refinement | 0.063 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.062 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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