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Information card for entry 4038973
Preview
Coordinates | 4038973.cif |
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Original paper (by DOI) | HTML |
Formula | C25 H31 Fe Mo2 O6 P |
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Calculated formula | C25 H31 Fe Mo2 O6 P |
Title of publication | Reactions of the unsaturated methyl-bridged complexes [Mo2Cp2(μ-CH3)(μ-P Bu2)(CO)x] (x = 1, 2) towards transition metal carbonyls: convenient dehydrogenative route to heterometallic methylidyne-bridged clusters |
Authors of publication | Alvarez, M. Angeles; Casado-Ruano, Melodie; García, M. Esther; García-Vivó, Daniel; Ruiz, Miguel A. |
Journal of publication | Journal of Organometallic Chemistry |
Year of publication | 2022 |
Journal volume | 959 |
Pages of publication | 122206 |
a | 17.3932 ± 0.0003 Å |
b | 17.6468 ± 0.0002 Å |
c | 18.7329 ± 0.0004 Å |
α | 90° |
β | 113.905 ± 0.002° |
γ | 90° |
Cell volume | 5256.55 ± 0.18 Å3 |
Cell temperature | 150 ± 0.1 K |
Ambient diffraction temperature | 150 ± 0.1 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0429 |
Residual factor for significantly intense reflections | 0.0364 |
Weighted residual factors for significantly intense reflections | 0.0877 |
Weighted residual factors for all reflections included in the refinement | 0.0918 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.029 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
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