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Information card for entry 4060076
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Coordinates | 4060076.cif |
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Original paper (by DOI) | HTML |
Chemical name | (pentamethylcyclopentadienyl)(triisopropylphosphine) (dimethylchlorosilyl)ruthenium dihydride |
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Formula | C21 H44 Cl P Ru Si |
Calculated formula | C21 H44 Cl P Ru Si |
Title of publication | Syntheses and X-ray Diffraction Studies of Half-Sandwich Hydridosilyl Complexes of Ruthenium |
Authors of publication | Osipov, Alexander L.; Gerdov, Sergei M.; Kuz'mina, Lyudmila G.; Howard, Judith A. K.; Nikonov, Georgii I. |
Journal of publication | Organometallics |
Year of publication | 2005 |
Journal volume | 24 |
Journal issue | 4 |
Pages of publication | 587 - 602 |
a | 13.849 ± 0.002 Å |
b | 9.9235 ± 0.0015 Å |
c | 17.759 ± 0.003 Å |
α | 90° |
β | 94.524 ± 0.003° |
γ | 90° |
Cell volume | 2432.9 ± 0.6 Å3 |
Cell temperature | 123 ± 2 K |
Ambient diffraction temperature | 123 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0566 |
Residual factor for significantly intense reflections | 0.0403 |
Weighted residual factors for significantly intense reflections | 0.104 |
Weighted residual factors for all reflections included in the refinement | 0.11 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.07 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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