Information card for entry 4060077

Structure parameters

• Chemical name: (pentamethylcyclopentadienyl)(diisopropylmethylphosphine) (dimethylchlorosilyl)ruthenium dihydride
• Formula: C19 H40 Cl P Ru Si
• Calculated formula: C19 H40 Cl P Ru Si
• Title of publication: Syntheses and X-ray Diffraction Studies of Half-Sandwich Hydridosilyl Complexes of Ruthenium
• Authors of publication: Osipov, Alexander L.; Gerdov, Sergei M.; Kuz'mina, Lyudmila G.; Howard, Judith A. K.; Nikonov, Georgii I.
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 4
• Pages of publication: 587 - 602
• a: 9.5522 ± 0.0003 Å
• b: 9.7988 ± 0.0003 Å
• c: 14.2729 ± 0.0005 Å
• α: 82.106 ± 0.001°
• β: 74.015 ± 0.001°
• γ: 63.171 ± 0.001°
• Cell volume: 1145.91 ± 0.06 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0468
• Residual factor for significantly intense reflections: 0.0452
• Weighted residual factors for significantly intense reflections: 0.1192
• Weighted residual factors for all reflections included in the refinement: 0.1207
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No