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Information card for entry 4060228
Preview
Coordinates | 4060228.cif |
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Original paper (by DOI) | HTML |
Chemical name | fac-[2-methoxycarbonylvinylbis(diphenylphosphanyl)methanide tricarbonyl tertbutylisocyanide manganese(I)] |
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Formula | C37 H34 Mn N O5 P2 |
Calculated formula | C37 H34 Mn N O5 P2 |
Title of publication | Metal-Assisted Regio- and Stereospecific Insertion of Alkynes into a C-H Bond, Leading to Functionalized Diphosphane Ligands |
Authors of publication | Javier Ruiz; Roberto Quesada; Víctor Riera; Eduardo Castellano; Oscar Piro |
Journal of publication | Organometallics |
Year of publication | 2004 |
Journal volume | 23 |
Pages of publication | 175 - 177 |
a | 18.821 ± 0.001 Å |
b | 18.95 ± 0.001 Å |
c | 19.487 ± 0.001 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 6950.2 ± 0.6 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 6 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.0586 |
Residual factor for significantly intense reflections | 0.0421 |
Weighted residual factors for significantly intense reflections | 0.1098 |
Weighted residual factors for all reflections included in the refinement | 0.1224 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.067 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4060228.html
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