Information card for entry 4060229

Structure parameters

• Formula: C22 H54 Al2 Mg2 O8
• Calculated formula: C20.11 H54 Al2 Mg2 O7.37
• Title of publication: Syntheses and Molecular Structure of [Mg2(OR)4(AlMe3)2] and [ZrCl3(OR)2(AlMe2)] (OR =1-methoxy-2-propoxide)
• Authors of publication: Józef Utko; Agnieszka Lizurek; Lucjan B. Jerzykiewicz; Piotr Sobota
• Journal of publication: Organometallics
• Year of publication: 2004
• Journal volume: 23
• Pages of publication: 296 - 298
• a: 8.155 ± 0.001 Å
• b: 22.599 ± 0.003 Å
• c: 9.644 ± 0.002 Å
• α: 90°
• β: 114.49 ± 0.01°
• γ: 90°
• Cell volume: 1617.4 ± 0.4 ų
• Cell temperature: 100 ± 1 K
• Ambient diffraction temperature: 100 ± 1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0853
• Residual factor for significantly intense reflections: 0.0643
• Weighted residual factors for significantly intense reflections: 0.1658
• Weighted residual factors for all reflections included in the refinement: 0.1791
• Goodness-of-fit parameter for all reflections included in the refinement: 1.088
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No