Information card for entry 4063232

Structure parameters

• Common name: [MgCl(thf)(mesNPPh2CHPPh2Nmes)].toluene
• Formula: C54 H59 Cl Mg N2 O P2
• Calculated formula: C54 H59 Cl Mg N2 O P2
• Title of publication: Synthesis and M-Cγ Hemilability of Group 2 Bis(phosphinimino)methanides
• Authors of publication: Shabana A. Ahmed; Michael S. Hill; Peter B. Hitchcock
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 2
• Pages of publication: 394 - 402
• a: 30.8401 ± 0.0002 Å
• b: 30.8401 ± 0.0002 Å
• c: 10.2288 ± 0.0001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9728.73 ± 0.13 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 82
• Hermann-Mauguin space group symbol: I -4
• Hall space group symbol: I -4
• Residual factor for all reflections: 0.047
• Residual factor for significantly intense reflections: 0.038
• Weighted residual factors for significantly intense reflections: 0.0831
• Weighted residual factors for all reflections included in the refinement: 0.0873
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No