Crystallography Open Database

Information card for entry 4063285

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Coordinates	4063285.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C39.5 H37.5 Cl6 P2 Pd
Calculated formula	C39.346 H36 Cl6.037 P2 Pd
Title of publication	Palladium Complexes Bearing Novel Strongly Bent Trans-Spanning Diphosphine Ligands: Synthesis, Characterization, and Catalytic Activity
Authors of publication	Olga Grossman; Clarit Azerraf; Dmitri Gelman
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	2
Pages of publication	375 - 381
a	12.0089 ± 0.0013 Å
b	12.6271 ± 0.0014 Å
c	15.4198 ± 0.0017 Å
α	67.5 ± 0.002°
β	74.016 ± 0.002°
γ	65.386 ± 0.002°
Cell volume	1945.1 ± 0.4 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0376
Residual factor for significantly intense reflections	0.0336
Weighted residual factors for significantly intense reflections	0.0925
Weighted residual factors for all reflections included in the refinement	0.0947
Goodness-of-fit parameter for all reflections included in the refinement	1.064
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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