Information card for entry 4063286

Structure parameters

• Formula: C35 H43 Cl13 P2 Pd2
• Calculated formula: C35 H40 Cl13 P2 Pd2
• Title of publication: Palladium Complexes Bearing Novel Strongly Bent Trans-Spanning Diphosphine Ligands: Synthesis, Characterization, and Catalytic Activity
• Authors of publication: Olga Grossman; Clarit Azerraf; Dmitri Gelman
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 2
• Pages of publication: 375 - 381
• a: 15.3648 ± 0.0009 Å
• b: 22.1329 ± 0.0012 Å
• c: 14.2719 ± 0.0008 Å
• α: 90°
• β: 106.938 ± 0.001°
• γ: 90°
• Cell volume: 4642.9 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0543
• Residual factor for significantly intense reflections: 0.0374
• Weighted residual factors for significantly intense reflections: 0.0892
• Weighted residual factors for all reflections included in the refinement: 0.0937
• Goodness-of-fit parameter for all reflections included in the refinement: 0.966
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No