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Information card for entry 4063399
Preview
Coordinates | 4063399.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C28 H49 N O2 Sn2 W |
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Calculated formula | C28 H49 N O2 Sn2 W |
SMILES | [W]1234(C#[O])(C#[O])(C#[N]C(C)(C)C)[c]5([cH]4[cH]3[cH]2[cH]15)[Sn]([Sn](C(C)(C)C)C(C)(C)C)(C(C)(C)C)C(C)(C)C |
Title of publication | Insertion vs Ligand Exchange: Reactivity of DistannaAnsaHalf-Sandwich Complexes of Molybdenum and Tungsten toward Isocyanide and Phosphine Complexes of Nickel and Palladium |
Authors of publication | Braunschweig, Holger; Dörfler, Rainer; Gruss, Katrin; Köhler, Julia; Radacki, Krzysztof |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 2 |
Pages of publication | 305 - 312 |
a | 10.953 ± 0.003 Å |
b | 14.23 ± 0.004 Å |
c | 22.311 ± 0.006 Å |
α | 85.601 ± 0.01° |
β | 80.273 ± 0.011° |
γ | 71.19 ± 0.009° |
Cell volume | 3243.5 ± 1.6 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0208 |
Residual factor for significantly intense reflections | 0.0176 |
Weighted residual factors for significantly intense reflections | 0.0545 |
Weighted residual factors for all reflections included in the refinement | 0.0698 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.32 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4063399.html
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Users of the data should acknowledge the original authors of the
structural data.