Information card for entry 4063400

Structure parameters

• Formula: C29 H55 O2 P Sn2 W
• Calculated formula: C29 H55 O2 P Sn2 W
• Title of publication: Insertion vs Ligand Exchange: Reactivity of DistannaAnsaHalf-Sandwich Complexes of Molybdenum and Tungsten toward Isocyanide and Phosphine Complexes of Nickel and Palladium
• Authors of publication: Braunschweig, Holger; Dörfler, Rainer; Gruss, Katrin; Köhler, Julia; Radacki, Krzysztof
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 2
• Pages of publication: 305 - 312
• a: 18.123 ± 0.0019 Å
• b: 11.6141 ± 0.0012 Å
• c: 16.1766 ± 0.0017 Å
• α: 90°
• β: 93.124 ± 0.002°
• γ: 90°
• Cell volume: 3399.8 ± 0.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0219
• Residual factor for significantly intense reflections: 0.0191
• Weighted residual factors for significantly intense reflections: 0.0457
• Weighted residual factors for all reflections included in the refinement: 0.0472
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No