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Information card for entry 4064039
Preview
Coordinates | 4064039.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C22 H34 Cl11 O Ru2 S Sb3 |
---|---|
Calculated formula | C22 H34 Cl11 O Ru2 S Sb3 |
SMILES | [Sb]12([Cl][Ru]345678([Ru]9%10%11%12([Cl]1)([Cl]3)([S]4O2)[c]1([c]%12([c]%11([c]%10([c]91C)C)C)C)CC)[c]1([c]5([c]6([c]7([c]81C)C)C)C)CC)(Cl)Cl.[Sb](Cl)(Cl)Cl.[Sb](Cl)(Cl)Cl |
Title of publication | Preparation of Incomplete Cubane-Type Ru2M(μ3-S)(μ2-Cl)3Clusters (M = Sb, Bi) and Isolation of the Ru2Sb Cluster Having a Novel μ3-SO Ligand. Functions in Oxygen Atom Transfer and Catalytic Oxidation of PPh3to O═PPh3by Molecular O2 |
Authors of publication | Oya, Kazumasa; Seino, Hidetake; Akiizumi, Midori; Mizobe, Yasushi |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 11 |
Pages of publication | 2939 |
a | 13.787 ± 0.003 Å |
b | 16.768 ± 0.003 Å |
c | 17.268 ± 0.003 Å |
α | 77.341 ± 0.005° |
β | 88.378 ± 0.006° |
γ | 87.547 ± 0.006° |
Cell volume | 3890.7 ± 1.3 Å3 |
Cell temperature | 293.1 K |
Ambient diffraction temperature | 293.1 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for significantly intense reflections | 0.0422 |
Weighted residual factors for all reflections included in the refinement | 0.1318 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.007 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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