Information card for entry 4064040

Structure parameters

• Formula: C38 H58 N3 O2 Si2 Ta
• Calculated formula: C38 H58 N3 O2 Si2 Ta
• Title of publication: Group 5 Metal Binaphtholate Complexes for Catalytic Asymmetric Hydroaminoalkylation and Hydroamination/Cyclization
• Authors of publication: Reznichenko, Alexander L.; Emge, Thomas J.; Audörsch, Stephan; Klauber, Eric G.; Hultzsch, Kai C.; Schmidt, Bernd
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 5
• Pages of publication: 921
• a: 10.7857 ± 0.0005 Å
• b: 15.5435 ± 0.0007 Å
• c: 11.9546 ± 0.0006 Å
• α: 90°
• β: 95.17 ± 0.001°
• γ: 90°
• Cell volume: 1996.01 ± 0.16 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0165
• Residual factor for significantly intense reflections: 0.0161
• Weighted residual factors for significantly intense reflections: 0.0386
• Weighted residual factors for all reflections included in the refinement: 0.0388
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No