Information card for entry 4065660

Structure parameters

• Formula: C49 H84 N O P3 Ru S2
• Calculated formula: C49 H81 N O P3 Ru S2
• Title of publication: Formation of a Ruthenium(II) Dicyclohexyl(η2-cyclohex-3-enyl)phosphine Hydride Complex from an Alkylidene Precursor
• Authors of publication: Cheung, Wai-Man; Chiu, Wai-Hang; Yi, Xiao-Yi; Zhang, Qian-Feng; Williams, Ian D.; Leung, Wa-Hung
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 8
• Pages of publication: 1981
• a: 18.3351 ± 0.0013 Å
• b: 14.4241 ± 0.001 Å
• c: 19.9515 ± 0.0014 Å
• α: 90°
• β: 109.697 ± 0.001°
• γ: 90°
• Cell volume: 4967.8 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0557
• Residual factor for significantly intense reflections: 0.038
• Weighted residual factors for significantly intense reflections: 0.081
• Weighted residual factors for all reflections included in the refinement: 0.0862
• Goodness-of-fit parameter for all reflections included in the refinement: 0.979
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No