Information card for entry 4065661

Structure parameters

• Formula: C30 H60 N P3 Ru S2
• Calculated formula: C30 H60 N P3 Ru S2
• SMILES: [RuH]123([S]=P(N=P(S1)(C(C)C)C(C)C)(C(C)C)C(C)C)[P](C1CCCCC1)(C1CCCCC1)C1C[CH]2=[CH]3CC1
• Title of publication: Formation of a Ruthenium(II) Dicyclohexyl(η2-cyclohex-3-enyl)phosphine Hydride Complex from an Alkylidene Precursor
• Authors of publication: Cheung, Wai-Man; Chiu, Wai-Hang; Yi, Xiao-Yi; Zhang, Qian-Feng; Williams, Ian D.; Leung, Wa-Hung
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 8
• Pages of publication: 1981
• a: 9.6266 ± 0.001 Å
• b: 11.5208 ± 0.0012 Å
• c: 16.9307 ± 0.0018 Å
• α: 95.784 ± 0.001°
• β: 102.749 ± 0.001°
• γ: 108.077 ± 0.001°
• Cell volume: 1711.8 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0283
• Residual factor for significantly intense reflections: 0.0239
• Weighted residual factors for significantly intense reflections: 0.0587
• Weighted residual factors for all reflections included in the refinement: 0.0602
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No