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Information card for entry 4065704
Preview
Coordinates | 4065704.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C34 H34 N Yb |
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Calculated formula | C34 H34 N Yb |
SMILES | [Yb]123456789%10%11(N([C]1(=[C]2([C]13=CC=CC=C1)c1ccccc1)c1ccccc1)C(C)(C)C)([cH]1[cH]4[cH]5[cH]6[cH]71)[cH]1[cH]8[cH]9[cH]%10[cH]%111 |
Title of publication | Insertion of Ketenimines into the Ln−C σ-Bond of Organolanthanides: A New Strategy for Synthesis of Lanthanide 1-Azaallyl Complexes |
Authors of publication | Zhang, Zhengxing; Bu, Xiuli; Zhang, Jie; Liu, Ruiting; Zhou, Xigeng; Weng, Linhong |
Journal of publication | Organometallics |
Year of publication | 2010 |
Journal volume | 29 |
Journal issue | 9 |
Pages of publication | 2111 |
a | 25.065 ± 0.007 Å |
b | 9.369 ± 0.003 Å |
c | 26.26 ± 0.008 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 6167 ± 3 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 4 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.0804 |
Residual factor for significantly intense reflections | 0.0382 |
Weighted residual factors for significantly intense reflections | 0.0821 |
Weighted residual factors for all reflections included in the refinement | 0.0858 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.005 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4065704.html
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Users of the data should acknowledge the original authors of the
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