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Information card for entry 4065705
Preview
Coordinates | 4065705.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C38 H42 N O Y |
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Calculated formula | C38 H42 N O Y |
SMILES | [Y]123456789%10%11(N([C]1(=[C]2([C]13=CC=CC=C1)c1ccccc1)c1ccccc1)C(C)(C)C)([cH]1[cH]4[cH]5[cH]6[cH]71)[cH]1[cH]8[cH]9[cH]%10[cH]%111.O1CCCC1 |
Title of publication | Insertion of Ketenimines into the Ln−C σ-Bond of Organolanthanides: A New Strategy for Synthesis of Lanthanide 1-Azaallyl Complexes |
Authors of publication | Zhang, Zhengxing; Bu, Xiuli; Zhang, Jie; Liu, Ruiting; Zhou, Xigeng; Weng, Linhong |
Journal of publication | Organometallics |
Year of publication | 2010 |
Journal volume | 29 |
Journal issue | 9 |
Pages of publication | 2111 |
a | 13.637 ± 0.004 Å |
b | 9.134 ± 0.003 Å |
c | 25.475 ± 0.008 Å |
α | 90° |
β | 98.862 ± 0.005° |
γ | 90° |
Cell volume | 3135.3 ± 1.7 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.1542 |
Residual factor for significantly intense reflections | 0.0729 |
Weighted residual factors for significantly intense reflections | 0.1586 |
Weighted residual factors for all reflections included in the refinement | 0.1905 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.004 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4065705.html
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Users of the data should acknowledge the original authors of the
structural data.