Information card for entry 4065755

Structure parameters

• Formula: C70 H66 Cl6 Ge2 O2
• Calculated formula: C70 H66 Cl6 Ge2 O2
• Title of publication: Reactions of Germenes with Somepara-Quinones: Formation of a Tricyclic Compound from 1,4-Benzoquinone Undergoing an Unexpected Rearrangement†
• Authors of publication: Ghereg, Dumitru; André, Erwan; Ech-Cherif El Kettani, Sakina; Saffon, Nathalie; Lazraq, Mohamed; Ranaivonjatovo, Henri; Gornitzka, Heinz; Miqueu, Karinne; Sotiropoulos, Jean-Marc; Escudié, Jean
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 21
• Pages of publication: 4849
• a: 8.8606 ± 0.0018 Å
• b: 10.974 ± 0.002 Å
• c: 16.164 ± 0.003 Å
• α: 91.254 ± 0.004°
• β: 101.916 ± 0.004°
• γ: 97.471 ± 0.004°
• Cell volume: 1522.9 ± 0.5 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0922
• Residual factor for significantly intense reflections: 0.0699
• Weighted residual factors for significantly intense reflections: 0.1711
• Weighted residual factors for all reflections included in the refinement: 0.1886
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No