Information card for entry 4065756

Structure parameters

• Formula: C73 H74 Cl2 Ge2 O2
• Calculated formula: C73 H74 Cl2 Ge2 O2
• Title of publication: Reactions of Germenes with Somepara-Quinones: Formation of a Tricyclic Compound from 1,4-Benzoquinone Undergoing an Unexpected Rearrangement†
• Authors of publication: Ghereg, Dumitru; André, Erwan; Ech-Cherif El Kettani, Sakina; Saffon, Nathalie; Lazraq, Mohamed; Ranaivonjatovo, Henri; Gornitzka, Heinz; Miqueu, Karinne; Sotiropoulos, Jean-Marc; Escudié, Jean
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 21
• Pages of publication: 4849
• a: 11.9661 ± 0.0003 Å
• b: 14.425 ± 0.0004 Å
• c: 17.8089 ± 0.0005 Å
• α: 86.197 ± 0.002°
• β: 85.504 ± 0.001°
• γ: 87.695 ± 0.001°
• Cell volume: 3055.91 ± 0.14 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1099
• Residual factor for significantly intense reflections: 0.0576
• Weighted residual factors for significantly intense reflections: 0.1172
• Weighted residual factors for all reflections included in the refinement: 0.1391
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No