Information card for entry 4066174

Structure parameters

• Formula: C27 H36 Cl3 N2 P
• Calculated formula: C27 H36 Cl3 N2 P
• Title of publication: Carbene-Stabilized Parent Phosphinidene†
• Authors of publication: Wang, Yuzhong; Xie, Yaoming; Abraham, Mariham Y.; Gilliard, Robert J.; Wei, Pingrong; Schaefer, Henry F.; Schleyer, Paul v. R.; Robinson, Gregory H.
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 21
• Pages of publication: 4778
• a: 10.6288 ± 0.0006 Å
• b: 13.9767 ± 0.0007 Å
• c: 19.8632 ± 0.0011 Å
• α: 90°
• β: 103.215 ± 0.001°
• γ: 90°
• Cell volume: 2872.6 ± 0.3 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1241
• Residual factor for significantly intense reflections: 0.0686
• Weighted residual factors for significantly intense reflections: 0.1901
• Weighted residual factors for all reflections included in the refinement: 0.2286
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No